反応式
[Pb:1]=O.[OH-].[Na+].[C:5]([OH:9])(=[O:8])[CH:6]=[CH2:7]>>[C:5]([O-:9])(=[O:8])[CH:6]=[CH2:7].[Pb+2:1].[C:5]([O-:9])(=[O:8])[CH:6]=[CH2:7]参加物
4
実験手順
111.5 gms of lead monoxide is taken in 0.1 NaOH and the mixture stirred in a round bottom flask for 30 minutes at room temperature, 72 gms of acrylic acid is then adding by a dropping funnel and a period of 1 hour. The mixture is heated under reflux conditions to 35° C. for 1 hour. The yield was 93% of lead acrylate after filtration, washing and drying.
後処理
- temperatureThe mixture is heated under reflux conditions to 35° C. for 1 hour
出典と根拠
- ORDレコード
- ord-2efc357025694a09b2d39f0e11906115
- 出典データセット
- uspto-grants-2012_05
- 特許番号
- US08173754B2
関連ノート
読み込み中…