Triethyl Citrate → Ethyl Acetoacetate
反応式
C(OCC)(=O)[CH2:2][C:3]([CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])(C(OCC)=O)[OH:4]>CC([O-])C.CC([O-])C.CC([O-])C.CC([O-])C.[Ti+4]>[C:11]([O:13][CH2:14][CH3:15])(=[O:12])[CH2:10][C:3]([CH3:2])=[O:4]参加物
3
実験手順
In the same way as in Example 1, 60 g (0.21 mol) of tetraisopropyl titanate were reacted with 116.6 g (0.42 mol) of triethyl citrate. The mixture was freed of alcohol under vacuum and 154.6 g of a clear, pale yellow liquid was obtained.
後処理
- customwas obtained
出典と根拠
- ORDレコード
- ord-0b1f2e1c0f294ff991c72bb3ca95134c
- 出典データセット
- uspto-grants-1995_06
- 特許番号
- US05428103
反応ノート
読み込み中…