Hydrogen Bromide → HCID 70576814、化合物

HRID 225306

反応式

HRID 225306 の反応式
[NH2:1][CH:2]([C:6]1[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][CH:7]=1)[C:3]([OH:5])=[O:4].[BrH:13].[CH2:14]=O>>[BrH:13].[NH2:1][CH:2]([C:6]1[CH:11]=[CH:10][C:9]([OH:12])=[C:8]([CH2:14][Br:13])[CH:7]=1)[C:3]([OH:5])=[O:4]

参加物

4

反応物 3

HCID 260Hydrogen Bromide2 回HCID 712FormaldehydeHCID 921434-Hydroxyphenylglycine

生成物 1

HCID 70576814HCID 70576814、化合物

実験手順

To a solution of (-)-α-amino-4-hydroxybenzeneacetic acid (0.6 mole) in a minimum amount of concentrated hydrobromic acid at 35°-40° C. is added 50 ml of aqueous formaldehyde (35-37%) (0.6 mole). The addition of hydrogen bromide gas is begun. After 5-10 minutes, a solid begins to precipitate. Stirring is continued for 30 minutes. The title compound is collected and washed with ether and acetone.

後処理

  1. customto precipitate
  2. waitis continued for 30 minutes
  3. customThe title compound is collected
  4. washwashed with ether and acetone

出典と根拠

ORDレコード
ord-bfac019684294d10844af47e66f9c982
出典データセット
uspto-grants-1980_11
特許番号
US04236002

関連ノート

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