反応式
[O-2].[Ca+2].[O-2].[Al+3].[O-2].[O-2].[Al+3].[CH2:8]([CH:10]1[CH2:15][CH2:14][CH2:13][CH2:12][CH:11]1[NH2:16])[CH3:9]>[Pd]>[CH2:8]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[NH2:16])[CH3:9]参加物
5
実験手順
The procedure described in Example 27 is followed, using a reaction temperature of 250° C. and a catalyst which contains 0.5% by weight of palladium on a mixture of 19.4% by weight of calcium oxide and 80.6% by weight of aluminum oxide, and starting from 2-ethylcyclohexylamine. o-Ethylaniline (boiling point=210° C.) is obtained in a yield of 95% of the theory.
後処理
- customa reaction temperature of 250° C.
出典と根拠
- ORDレコード
- ord-7047ce36165548e0b0dda930a92fa923
- 出典データセット
- uspto-grants-1984_01
- 特許番号
- US04429155
関連ノート
読み込み中…