Isopropylamine → HCID 86699881、化合物

HRID 333043

反応式

HRID 333043 の反応式
[CH3:1][C:2]([CH3:9])([CH2:5][N:6]([CH3:8])[CH3:7])[CH:3]=O.CC(N)C.[NH2:14][CH2:15][CH2:16][CH2:17][Si:18]([O:23][CH3:24])([O:21][CH3:22])[O:19][CH3:20]>>[CH3:1][C:2]([CH3:9])([CH2:5][N:6]([CH3:8])[CH3:7])[CH:3]=[N:14][CH2:15][CH2:16][CH2:17][Si:18]([O:23][CH3:24])([O:19][CH3:20])[O:21][CH3:22]

参加物

4

反応物 3

HCID 6363IsopropylamineHCID 83756AminopropyltrimethoxysilaneHCID 849212,2-Dimethyl-3-(dimethylamino)propionaldehyde

生成物 1

HCID 86699881HCID 86699881、化合物

実験手順

13.57 g 2,2-dimethyl-3-dimethylaminopropanal, 7.45 g 2-propanamine and 17.93 g 3-aminopropyltrimethoxysilane were reacted according to the general manufacturing procedure (iminosilanes). The product was distilled after manufacture in order to remove oligomer portions. Yield: 28.4 g of a clear, colorless oil having an amine content of 6.61 mmol N/g and a purity of 95%.

後処理

  1. distillationThe product was distilled after manufacture in order
  2. customto remove oligomer portions

出典と根拠

ORDレコード
ord-03e3e68b4236413386c8ac136302706a
出典データセット
uspto-grants-2014_11
特許番号
US08877955B2

関連ノート

読み込み中…