Diisopropylethylamine → N-(3-Amino-4-thienyl)-N'-(2,6-dimethylphenyl)thiourea
反応式
C(N(C(C)C)C(C)C)C.Br.Br.[NH2:12][C:13]1[C:17]([NH2:18])=[CH:16][S:15][CH:14]=1.[CH3:19][C:20]1[CH:25]=[CH:24][CH:23]=[C:22]([CH3:26])[C:21]=1[N:27]=[C:28]=[S:29]>C1COCC1>[NH2:12][C:13]1[C:17]([NH:18][C:28]([NH:27][C:21]2[C:20]([CH3:19])=[CH:25][CH:24]=[CH:23][C:22]=2[CH3:26])=[S:29])=[CH:16][S:15][CH:14]=1参加物
5
実験手順
was obtained in a similar manner to the method specified in Example 6a) by reacting a mixture prepared from 0.74 g of N-ethyl-N,N-diisopropylamine in 40 ml of THF, 0.8 g of 3,4-diaminothiophene dihydrobromide and 0.47 g of 2,6-dimethylphenyl isothiocyanate.
後処理
- customwas obtained in a similar manner to the method
出典と根拠
- ORDレコード
- ord-55ab235eef0b408d86fc24fc8d6b7ba4
- 出典データセット
- uspto-grants-2007_02
- 特許番号
- US07179830B2
反応ノート
読み込み中…