Sodium Iodide → HCID 66732740、化合物

HRID 389002

反応式

HRID 389002 の反応式
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1.[I-].[Na+].[OH-].[Na+].Cl[CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][OH:27]>O>[C:3]1([C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][CH:13]=2)[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=1[O:1][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][OH:27]

参加物

6

反応物 4

HCID 5238Sodium IodideHCID 7017(1,1'-Biphenyl)-2-olHCID 14798Sodium HydroxideHCID 900121-Octanol, 8-chloro-

生成物 1

HCID 66732740HCID 66732740、化合物

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

The compound was prepared using essentially the procedure of Preparatory Example 1 with 2-hydroxy biphenyl (40 g.), water (250 g.), sodium iodide (3.5 g.) and sodium hydroxide (37.6 g. of 50% in water). This mixture was heated to 100° C. with agitation and 8-chloro-1-octanol (77.4 g.) was added. The product was recovered essentially as in Preparatory Example 1.

後処理

  1. customThe compound was prepared
  2. additionwas added
  3. customThe product was recovered essentially as in Preparatory Example 1

出典と根拠

ORDレコード
ord-05054416c02248f89e5b132dca5599b6
出典データセット
uspto-grants-2013_02
特許番号
US08378046B2

関連ノート

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