反応式
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[C:7]([Cl:9])[CH:8]=1)[NH2:5].[CH2:10](C(=O)C([O-])=O)[CH3:11].[CH3:17][CH:18]=[CH:19][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1.F[C:27](F)(F)[C:28]([OH:30])=[O:29]>C(#N)C>[CH2:10]([O:30][C:28]([CH:27]1[CH:18]([CH3:17])[CH:19]([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)[C:3]2[C:4](=[CH:6][C:7]([Cl:9])=[CH:8][C:2]=2[Cl:1])[NH:5]1)=[O:29])[CH3:11]参加物
6
実験手順
Compound 42 was prepared by the basic process from 5.0 mmol 3,5-dichloroaniline, 5.5 mmol ethylglyoxalate solution (50% toluene), 15.0 mmol β-methylstyrene and 5.0 mmol trifluoroacetic acid in 30.0 ml acetonitrile.
出典と根拠
- ORDレコード
- ord-834b71bf6a504cfa994a60174df21e7d
- 出典データセット
- uspto-grants-2004_03
- 特許番号
- US06699877B2
関連ノート
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