反応式
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[C:7]([Cl:9])[CH:8]=1)[NH2:5].[CH2:10](C(=O)C([O-])=O)[CH3:11].[C:17]1([O:26][CH3:27])[CH:25]=[CH:24][C:20]([CH:21]=[CH:22][CH3:23])=[CH:19][CH:18]=1.F[C:29](F)(F)[C:30]([OH:32])=[O:31]>C(#N)C>[CH2:10]([O:32][C:30]([CH:29]1[CH:22]([CH3:23])[CH:21]([C:20]2[CH:24]=[CH:25][C:17]([O:26][CH3:27])=[CH:18][CH:19]=2)[C:3]2[C:4](=[CH:6][C:7]([Cl:9])=[CH:8][C:2]=2[Cl:1])[NH:5]1)=[O:31])[CH3:11]参加物
6
実験手順
Compound 45 was prepared by the basic process from 5.0 mmol 3,5-dichloroaniline, 5.5 mmol ethylglyoxalate solution (50% toluene), 15.0 mmol anethole and 5.0 mmol trifluoroacetic acid in 30.0 ml acetonitrile.
出典と根拠
- ORDレコード
- ord-37f150e1e231435eabe8bc0580b12d1c
- 出典データセット
- uspto-grants-2004_03
- 特許番号
- US06699877B2
関連ノート
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