Acetonitrile → Disodium adipate

HRID 616621

反応式

HRID 616621 の反応式
[C:1]([O:11]C)(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O:8]C)=[O:7].C(#N)C.[OH-].[Na+:17]>O>[C:1]([O-:11])(=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([O-:8])=[O:7].[Na+:17].[Na+:17]

参加物

5

反応物 3

HCID 6342AcetonitrileHCID 12329DimethyladipateHCID 14798Sodium Hydroxide

生成物 1

HCID 24073Disodium adipate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

17.4 Grams (0.1 mole) of dimethyl adipate are dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 Grams (0.2 mole) of sodium hydroxide dissolved in 6.0 g. of water are added to the reaction mixture. The reaction mixture is stirred at reflux temperature for 18 hours. The resulting solution is filtered hot and the solids are air dried to yield disodium adipate as the reaction product.

後処理

  1. temperatureat reflux temperature for 18 hours
  2. filtrationThe resulting solution is filtered hot
  3. customdried

出典と根拠

ORDレコード
ord-4a44ab5cc5df4d7eaf36af8930e8ae52
出典データセット
uspto-grants-1978_02
特許番号
US04075234

関連ノート

読み込み中…