Formaldehyde → Melamine formaldehyde

HRID 648137ノート

反応式

HRID 648137 の反応式
C(C1=C[C:11](OC1=O)=[O:12])=CC1C=CC=CC=1.[Na].[N:17]1[C:24]([NH2:25])=[N:23][C:21]([NH2:22])=[N:20][C:18]=1[NH2:19].C=O.[OH-].[Na+]>C1(C(C2C=CC=CC=2)C)C=CC=CC=1.O>[CH2:11]=[O:12].[N:17]1[C:24]([NH2:25])=[N:23][C:21]([NH2:22])=[N:20][C:18]=1[NH2:19]

参加物

8

反応物 5

HCID 712FormaldehydeHCID 7955MelamineHCID 14798Sodium HydroxideHCID 5360545SodiumHCID 54215275Styrenemaleic anhydride

生成物 1

HCID 93374Melamine formaldehyde

試薬・触媒・溶媒 2

HCID 962Water溶媒HCID 119181,1-Diphenylethane溶媒

反応条件

温度
60 °C

実験手順

Thus, 80 parts of a solution of 3.5 parts of crystal violet lactone (CVL) and 1.5 parts of benzoyl leucomethylene blue (BLMB) in 1,1-diphenylethane was added to 100 parts of 5% aqueous solution of styrenemaleic anhydride copolymer containing a small quantity of sodium hdyroxide and having a pH value of 4.0, and emulsified to give an emulsion. On the other hand, a mixture comprising 10 parts of melamine, 25 parts of 37% aqueous solution of formaldehyde and 65 parts of water was adjusted to pH 9.0 with sodium hydroxide and heated to 60° C. The mixture became transparent in 15 minutes, and there was obtained a melamine-formaldehyde pre-condensate. The pre-condensate was added to the above-mentioned emulsion, the temperature was adjusted to 60° C. and stirring was continued. The formation of capsules was confirmed in 30 minutes, after which the mixture was cooled to room temperature. The microcapsule-containing dispersion thus obtained had a solid content of about 45%.

後処理

  1. customto give an emulsion

出典と根拠

ORDレコード
ord-87668fcf8f974f96ba029920bbab9f2d
出典データセット
uspto-grants-1983_10
特許番号
US04411451

反応ノート

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