反応式
[F:1][C:2]([F:15])([F:14])[S:3]([O:6]S(C(F)(F)F)(=O)=O)(=[O:5])=[O:4].[C:16](=O)(OC)OC>>[F:1][C:2]([F:15])([F:14])[S:3]([O:6][CH3:16])(=[O:5])=[O:4]参加物
3
実験手順
731 g (2.59 mol) of trifluoromethanesulfonic anhydride and 232 g (2.58 mol) of dimethyl carbonate are added to the residue, and the process described above is repeated. 837 g of methyl trifluoromethanesulfonate having a purity of greater than 99% are isolated (yield: 99.1%).
出典と根拠
- ORDレコード
- ord-befbfb3aff7c451d95620ddeb9864f61
- 出典データセット
- uspto-grants-2006_08
- 特許番号
- US07084290B2
関連ノート
読み込み中…