Methacrylic Acid → Methacrylic acid hydroxypropyl methacrylate

HRID 747812

反応式

HRID 747812 の反応式
C1COCC1.[C:6]([OH:11])(=[O:10])[C:7]([CH3:9])=[CH2:8].[C:12]([O:17][CH2:18][CH2:19][CH2:20][OH:21])(=[O:16])[C:13]([CH3:15])=[CH2:14]>C(C(OC(CC)(CC)C)(CC)C)C.CC(N=NC(C#N)(C)C)(C#N)C>[C:6]([OH:11])(=[O:10])[C:7]([CH3:9])=[CH2:8].[C:12]([O:17][CH2:18][CH2:19][CH2:20][OH:21])(=[O:16])[C:13]([CH3:15])=[CH2:14]

参加物

6

反応物 3

HCID 4093Methacrylic AcidHCID 8028TetrahydrofuranHCID 176943-Hydroxypropyl methacrylate

生成物 1

HCID 86602182Methacrylic acid hydroxypropyl methacrylate収率 582.3%

試薬・触媒・溶媒 2

HCID 6547Azobisisobutyronitrile触媒HCID 12430074Diethylethylether溶媒

実験手順

To 20 g of THF were added 9 g of methacrylic acid, 1 g of hydroxypropyl methacrylate, and 0.1 g of AIBN. The resulting mixture was reacted at 67° C. for 3 hours. After reaction, the resulting solution was dropped in diethylethyl ether, thereby obtaining 9.3 g of a photoresist polymer of Formula (IVd).

後処理

  1. customThe resulting mixture was reacted at 67° C. for 3 hours
  2. customAfter reaction

出典と根拠

ORDレコード
ord-a4dcbc86eb9c458dae976a088d9d0c1d
出典データセット
uspto-grants-2008_07
特許番号
US07399570B2

関連ノート

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