4-(Octyloxy)benzoic acid → 4-Octyloxybenzoyl chloride
反応式
S(Cl)([Cl:3])=O.[CH2:5]([O:13][C:14]1[CH:22]=[CH:21][C:17]([C:18](O)=[O:19])=[CH:16][CH:15]=1)[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]>>[CH2:5]([O:13][C:14]1[CH:22]=[CH:21][C:17]([C:18]([Cl:3])=[O:19])=[CH:16][CH:15]=1)[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]参加物
3
実験手順
A large excess of thionyl chloride was added to 10 g of the p-octyloxybenzoic acid prepared in (1), and the mixture was refluxed for 5 hours. Excessive thionyl chloride was distilled off to give a crude end compound.
後処理
- temperaturethe mixture was refluxed for 5 hours
- distillationExcessive thionyl chloride was distilled off
- customto give a crude end compound
出典と根拠
- ORDレコード
- ord-89aff4b1c18042e4bbb1f88ebba96f86
- 出典データセット
- uspto-grants-1998_03
- 特許番号
- US05723069
反応ノート
読み込み中…