2,3-Dinitrophenol → Sodium dinitrophenolate

HRID 874859

反応式

HRID 874859 の反応式
[N+:1]([C:4]1[C:5]([N+:11]([O-:13])=[O:12])=[C:6]([OH:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[H-].[Na+:15]>C1COCC1>[N+:1]([C:4]1[C:5]([N+:11]([O-:13])=[O:12])=[C:6]([O-:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[Na+:15]

参加物

4

反応物 2

HCID 61912,3-DinitrophenolHCID 24758Sodium hydride

生成物 1

HCID 86649331Sodium dinitrophenolate

試薬・触媒・溶媒 1

HCID 8028Tetrahydrofuran溶媒

実験手順

The anhydrous dinitrophenol (10.0 g, 54.3 mmol) was dissolved in anhydrous THF (300 mL) and then NaH(1.30 g, 54.3 mmol) was added slowly. After the solution was stirred for 3 hrs, solvent was removed under the reduced pressure to obtain 100 mol % sodium dinitrophenolate.

後処理

  1. customsolvent was removed under the reduced pressure

出典と根拠

ORDレコード
ord-d8af27706dff4fbb87b4281472467d2c
出典データセット
uspto-grants-2015_03
特許番号
US08981043B2

関連ノート

読み込み中…