2,3-Dinitrophenol → Sodium dinitrophenolate
反応式
[N+:1]([C:4]1[C:5]([N+:11]([O-:13])=[O:12])=[C:6]([OH:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[H-].[Na+:15]>C1COCC1>[N+:1]([C:4]1[C:5]([N+:11]([O-:13])=[O:12])=[C:6]([O-:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[Na+:15]参加物
4
実験手順
The anhydrous dinitrophenol (10.0 g, 54.3 mmol) was dissolved in anhydrous THF (300 mL) and then NaH (1.30 g, 54.3 mmol) was added slowly. After the solution was stirred for 3 hrs, solvent was removed under the reduced pressure to obtain 100 mol % sodium dinitrophenolate.
後処理
- customsolvent was removed under the reduced pressure
出典と根拠
- ORDレコード
- ord-bb64b922e5af466a87709b09e9ad12cb
- 出典データセット
- uspto-grants-2015_03
- 特許番号
- US08987411B2
反応ノート
読み込み中…