Ethanol → Ganex E 535

HRID 894306

反応式

HRID 894306 の反応式
C(O)C.[OH-].[Na+].[CH:6]([N:8]1[CH2:12][CH2:11][CH2:10][C:9]1=[O:13])=[CH2:7].[C:14]([O:17][CH:18]=[CH2:19])(=[O:16])[CH3:15]>C(OCC)C>[CH:6]([N:8]1[CH2:12][CH2:11][CH2:10][C:9]1=[O:13])=[CH2:7].[C:14]([O:17][CH:18]=[CH2:19])(=[O:16])[CH3:15]

参加物

6

反応物 4

HCID 702EthanolHCID 6917N-vinyl-2-pyrrolidoneHCID 7904Vinyl AcetateHCID 14798Sodium Hydroxide

生成物 1

HCID 270885Ganex E 535収率 95%

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒

反応条件

温度
30 °C

実験手順

Into a 2 liter round bottom flask 800 ml of ethanol, 12.8 g of sodium hydroxide pellets and 80 g of a copolymer composed of 70% N-vinylpyrrolidone and 30% vinyl acetate are introduced. The resulting reaction mixture is maintained with stirring at 30° C. for 2 hours and is then poured into 8 liters of diethyl ether to precipitate the desired polymer. After filtration the polymer is dried under reduced pressure. Yield: 95%.

後処理

  1. additionare introduced
  2. customThe resulting reaction mixture
  3. temperatureis maintained
  4. customto precipitate the desired polymer
  5. filtrationAfter filtration the polymer
  6. customis dried under reduced pressure

出典と根拠

ORDレコード
ord-89a3e98d71a44dd59f10265f058e1e6b
出典データセット
uspto-grants-1981_08
特許番号
US04283384

関連ノート

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