Ethanol → HCID 69639835, 화합물

HRID 1246586

반응식

HRID 1246586 반응식
[Na].C(O)C.[NH2:5][C:6]1[CH:16]=[CH:15][C:9]([C:10]([O:12][CH2:13][CH3:14])=[O:11])=[CH:8][CH:7]=1.[CH3:17][CH:18]([CH2:22][C:23]([CH3:26])([CH3:25])[CH3:24])CCO>C1CCCCC1>[NH2:5][C:6]1[CH:7]=[CH:8][C:9]([C:10]([O:12][CH2:13][CH2:14][CH:18]([CH3:17])[CH2:22][C:23]([CH3:26])([CH3:25])[CH3:24])=[O:11])=[CH:15][CH:16]=1

참가 물질

6

반응물 4

HCID 702Ethanol2회HCID 2337BenzocaineHCID 189383,5,5-Trimethyl-1-hexanolHCID 5360545Sodium

생성물 1

HCID 69639835HCID 69639835, 화합물

시약·촉매·용매 1

HCID 8078Cyclohexane용매

실험 절차

Sodium metal (1 g cat.) was added to ethanol (30 mL) to give a solution which was added to a suspension of ethyl 4-aminobenzoate (175 g, 1.06 mol) and 3,5,5 trimethyl hexanol (200 g, 1.4 mol) in cyclohexane (300 mL). The suspension was heated under reflux for 24 hours with the azeotropic removal of ethanol.

후처리

  1. customto give a solution which
  2. temperatureThe suspension was heated

출처 및 근거

ORD 기록
ord-74ff96502e7f4c339282b0b43bcc57c1
출처 데이터셋
uspto-grants-2006_10
특허 번호
US07129204B2

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