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OP([O-])(O)=O.[K+].OP([O-])([O-])=O.[K+].[K+].C[C@@H]([C@@H:21]1[C@@:25]2([CH3:43])[C@@H:26](O)[CH2:27][C@@H:28]3[C@@:33]4([CH3:39])[CH2:34][CH2:35][C@@H:36]([OH:38])[CH2:37][C@H:32]4[CH2:31][C@@H:30](O)[C@@:29]3(C)[C@@H:24]2[CH2:23][CH2:22]1)CCC([O-])=O.[Na+].CCC(CO[C:52]([C:65](N(CC[NH+](C)C)C)=O)([C:59]1C=CC=CC=1)[C:53]1C=[CH:57][CH:56]=[CH:55][CH:54]=1)CC.[Cl-].CC1N(C)N(C2C=CC=CC=2)C(=O)C=1N.C1(O)C=CC=CC=1>C(O)C.O>[CH3:59][CH:52]([CH2:53][CH2:54][CH2:55][C@H:56]([C@@H:24]1[C@:25]2([CH3:43])[C@H:21]([C@H:29]3[C@H:28]([CH2:27][CH2:26]2)[C@:33]2([CH3:39])[C:34]([CH2:35][C@H:36]([CH2:37][CH2:32]2)[OH:38])=[CH:31][CH2:30]3)[CH2:22][CH2:23]1)[CH3:57])[CH3:65]참가 물질
9
반응물 6
HCID 996Phenol
HCID 21514-Aminoantipyrine
HCID 19153X 100
HCID 24450Potassium Phosphate, Dibasic
HCID 516951Monobasic potassium phosphate
HCID 44582063sodium (4R)-4-[(3R,5S,7R,8R,9R,10S,12S,13R,14R,17R)-3,7,12-trihydroxy-8,10,13-trimethyl-1,2,3,4,5,6,7,9,11,12,14,15,16,17-tetradecahydrocyclopenta[a]phenanthren-17-yl]pentanoate생성물 1
시약·촉매·용매 2
실험 절차
In a 250 ml flask, a reaction mixture (designated "mixture A") was prepared by adding to 90 ml of distilled water the following: 1.497 g (KH2PO4 ; 1.568 g K2HPO4 ; 0.431 g. sodium cholate; 1.05 ml of a 25% solution of an alkylphenoxypolyethoxy ethanol, commercially available from Rohm and Haas Co., Philadelphia, Pa., under the trade designation Triton X-100; 0.0169 g 4-aminoantipyrine (used as a chromogen); and 0.145 ml phenol (10 M). Sufficient distilled water was added to make a final volume of 100 ml.
후처리
- customIn a 250 ml flask, a reaction mixture (designated
- custom"mixture A") was prepared
- distillationSufficient distilled water
- additionwas added
출처 및 근거
- ORD 기록
- ord-ed5a26d05eb249218272871db3a6f1ae
- 출처 데이터셋
- uspto-grants-1981_03
- 특허 번호
- US04259440
연결된 노트
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