Hydrochloric Acid → Tri-n-butylphosphonium tetraphenylborate

HRID 13868

반응식

HRID 13868 반응식
[CH2:1]([P:5]([CH2:10][CH2:11][CH2:12][CH3:13])[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].Cl.[C:15]1([B-:21]([C:34]2[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=2)([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.[Na+]>>[C:34]1([B-:21]([C:15]2[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=2)([C:22]2[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=2)[C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)[CH:35]=[CH:36][CH:37]=[CH:38][CH:39]=1.[CH2:10]([PH+:5]([CH2:1][CH2:2][CH2:3][CH3:4])[CH2:6][CH2:7][CH2:8][CH3:9])[CH2:11][CH2:12][CH3:13]

참가 물질

4

반응물 3

HCID 313Hydrochloric AcidHCID 13831TributylphosphineHCID 2723787Sodium Tetraphenylborate

생성물 1

HCID 23136640Tri-n-butylphosphonium tetraphenylborate수율 53%

실험 절차

Tri-n-butylphosphine is reacted with hydrochloric acid in the presence of sodium tetraphenylborate to produce tri-n-butylphosphonium tetraphenylborate (53% yield) (see Nonpatent Document 6).

출처 및 근거

ORD 기록
ord-0b6a244a31ae4bdea68240493807b244
출처 데이터셋
uspto-grants-2010_06
특허 번호
US07728176B2

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