Hydrochloric Acid → HCID 70274422, 화합물

HRID 1586847노트

반응식

HRID 1586847 반응식
[CH3:1][CH2:2][CH:3]([S:6]([NH2:9])(=[O:8])=[O:7])[CH2:4][CH3:5].[OH-].[Na+].[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([N:19]=[C:20]=[O:21])=[CH:15][CH:14]=1.Cl>CC(C)=O.O>[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([NH:19][C:20]([NH:9][S:6]([CH:3]([CH2:4][CH3:5])[CH2:2][CH3:1])(=[O:8])=[O:7])=[O:21])=[CH:15][CH:14]=1

참가 물질

7

반응물 4

HCID 313Hydrochloric AcidHCID 76934-Chlorophenyl IsocyanateHCID 14798Sodium HydroxideHCID 22131302Pentane-3-sulfonamide

생성물 1

HCID 70274422HCID 70274422, 화합물

시약·촉매·용매 2

HCID 180Acetone용매3회HCID 962Water용매

실험 절차

The general method of procedure A was followed with 3-pentanesulfonamide (10 g), acetone (300 ml), 1N sodium hydroxide (56 ml), and 4-chlorophenyl isocyanate (9.6 g) dissolved in 70 ml of acetone. After two hours of stirring, 1N HCl (66 ml) was added followed by more water. The acetone was stripped off, and the resulting solid collected, to give, after drying at 65° C. under vacuum, 13.1 g of product.

후처리

  1. customthe resulting solid collected
  2. customto give
  3. dry with materialafter drying at 65° C. under vacuum, 13.1 g of product

출처 및 근거

ORD 기록
ord-1a109a0adc0042daaa6e9855e6b21845
출처 데이터셋
uspto-grants-1993_06
특허 번호
US05216026

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