홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Hydrochloric Acid → N-(4-chlorophenyl)-N'-1-hexanesulfonylurea

HRID 1586851
노트
인쇄 미리보기

반응식

HRID 1586851 반응식
[CH2:1]([S:7]([NH2:10])(=[O:9])=[O:8])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[OH-].[Na+].[Cl:13][C:14]1[CH:19]=[CH:18][C:17]([N:20]=[C:21]=[O:22])=[CH:16][CH:15]=1.Cl>CC(C)=O>[Cl:13][C:14]1[CH:19]=[CH:18][C:17]([NH:20][C:21]([NH:10][S:7]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])(=[O:9])=[O:8])=[O:22])=[CH:16][CH:15]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

6

반응물 4

HCID 313Hydrochloric AcidHCID 76934-Chlorophenyl IsocyanateHCID 14798Sodium HydroxideHCID 13537577Hexane-1-sulfonamide

생성물 1

HCID 22131301N-(4-chlorophenyl)-N'-1-hexanesulfonylurea수율 87.6%

시약·촉매·용매 1

HCID 180Acetone용매2회
이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트

실험 절차

The general method of procedure A was followed with hexanesulfonamide (10 g), acetone (200 ml), 1N sodium hydroxide (60 ml), and 4-chlorophenyl isocyanate (8.8 g) in acetone (50 ml). After three hours of stirring, 1N HCl (60 ml) was added followed by removal of acetone and collection of solid from the water. The solid was washed with water and dried at 65° C. under vacuum to provide 16 g of product.

후처리

  1. customfollowed by removal of acetone and collection of solid from the water
  2. washThe solid was washed with water
  3. customdried at 65° C. under vacuum

출처 및 근거

ORD 기록
ord-81a26b394cd1474f8501f7424469659c
출처 데이터셋
uspto-grants-1993_06
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05216026

반응 노트

불러오는 중…