Hydrochloric Acid → HCID 372723, 화합물

HRID 1645406노트

반응식

HRID 1645406 반응식
[O-][Mn](=O)(=O)=O.[K+].[ClH:7].O.[CH2:9]1[S:17](=[O:19])(=[O:18])[O:16][CH2:15][CH2:14][O:13][S:10]1(=[O:12])=[O:11]>[OH-].[Na+]>[Cl:7][CH:9]1[S:10](=[O:11])(=[O:12])[O:13][CH2:14][CH2:15][O:16][S:17]1(=[O:19])=[O:18]

참가 물질

6

반응물 4

HCID 313Hydrochloric AcidHCID 962WaterHCID 57513CyclodisoneHCID 516875Potassium Permanganate

생성물 1

HCID 372723HCID 372723, 화합물

시약·촉매·용매 1

HCID 14798Sodium Hydroxide용매2회

실험 절차

A solution of 1.25 g of KMnO4 and 7.8 mL of conc. HCl in 115 mL of ice cooled H2O was stirred for 2 hrs. To this solution was added 2.02 g of ethylene methanedisulfonate in 25 mL of 0.5 molar NaOH. The solid obtained after acidification was placed in 15 mL of 0.5 M NaOH and the filtrate acidified to give 1.1 g of ethylene chloromethanedisulfonate, m.p. 85-88° C. (91-6).

후처리

  1. customThe solid obtained after acidification

출처 및 근거

ORD 기록
ord-22d6ed5cbbcf46878231f07a8ee090bb
출처 데이터셋
uspto-grants-2012_02
특허 번호
US08124793B2

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