M-Cresol → Cresentyl

HRID 2248529노트

반응식

HRID 2248529 반응식
[CH:1]1[C:6]([OH:7])=[CH:5][CH:4]=[CH:3][C:2]=1[CH3:8].[C:9](Cl)(=[O:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>[OH-].[Na+]>[C:9]([O:7][C:6]1[CH:5]=[CH:4][CH:3]=[C:2]([CH3:8])[CH:1]=1)(=[O:16])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

참가 물질

4

반응물 2

HCID 342M-CresolHCID 7412Benzoyl chloride

생성물 1

HCID 69193Cresentyl

시약·촉매·용매 1

HCID 14798Sodium Hydroxide용매

실험 절차

Metacresyl benzoate was prepared by vigorously shaking a mixture of metacresol (1 equivalent, 5 grams) and benzoyl chloride (1.2 equivalents, 7.1 grams) in a 10% aqueous solution of sodium hydroxide (100 ml) in a stoppered flask for 15 minutes. The white crystalline solid thus formed was removed by filtration, washed with water and dried to yield metacresyl benzoate.

후처리

  1. customMetacresyl benzoate was prepared
  2. customThe white crystalline solid thus formed
  3. customwas removed by filtration
  4. washwashed with water
  5. customdried

출처 및 근거

ORD 기록
ord-ba7d5364089d403682484ba65b5e582d
출처 데이터셋
uspto-grants-1991_08
특허 번호
US05041169

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