홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Hydrochloric Acid → HCID 17816498, 화합물

HRID 2249634
노트
인쇄 미리보기

반응식

HRID 2249634 반응식
[CH2:1]([O:6][C:7]1[CH:8]=[C:9]([CH:33]=[CH:34][C:35]=1[O:36][CH2:37][CH2:38][CH:39]([CH3:41])[CH3:40])[C:10]([C:12]1[CH:13]=[CH:14][C:15]([O:27][CH2:28][CH2:29][CH:30]([CH3:32])[CH3:31])=[C:16]([CH2:18][C:19]([O:21]CCC(C)C)=[O:20])[CH:17]=1)=[O:11])[CH2:2][CH:3]([CH3:5])[CH3:4].[OH-].[Na+].C(Cl)(Cl)Cl.Cl>C(O)C.O>[CH2:1]([O:6][C:7]1[CH:8]=[C:9]([CH:33]=[CH:34][C:35]=1[O:36][CH2:37][CH2:38][CH:39]([CH3:41])[CH3:40])[C:10]([C:12]1[CH:13]=[CH:14][C:15]([O:27][CH2:28][CH2:29][CH:30]([CH3:31])[CH3:32])=[C:16]([CH2:18][C:19]([OH:21])=[O:20])[CH:17]=1)=[O:11])[CH2:2][CH:3]([CH3:4])[CH3:5]
참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트

참가 물질

7

반응물 4

HCID 313Hydrochloric AcidHCID 6212ChloroformHCID 14798Sodium HydroxideHCID 17816502HCID 17816502, 화합물

생성물 1

HCID 17816498HCID 17816498, 화합물수율 83.6%

시약·촉매·용매 2

HCID 702Ethanol용매
HCID 962
Water
용매

반응 조건

온도
50 °C

실험 절차

In 12 ml of ethanol is dissolved 1.20 g of isopentyl 2-[5-(3,4-diisopentyloxybenzoyl)-2-isopentyloxyphenyl]acetate. After adding 0.6 ml of 5 mol/L aqueous solution of sodium hydroxide, the mixture is stirred at 50° C. for one hour. Chloroform and water are added to the reaction mixture, pH is adjusted to 2 with 6 mol/L hydrochloric acid, and the organic layer is separated. The organic layer is washed with water and saturated aqueous solution of sodium chloride successively, and the solvent is distilled off from the reaction mixture under reduced pressure. Thus, 0.88 g of 2-[5-(3,4-diisopentyloxybenzoyl)-2-isopentyloxyphenyl]acetic acid is obtained as a white solid product.

후처리

  1. customthe organic layer is separated
  2. washThe organic layer is washed with water and saturated aqueous solution of sodium chloride successively
  3. distillationthe solvent is distilled off from the reaction mixture under reduced pressure

출처 및 근거

ORD 기록
ord-0d1fa8255e9e4ccfa2891c9fc4b3c550
출처 데이터셋
uspto-grants-2008_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US07314888B1

반응 노트

불러오는 중…

이 페이지에서참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트