Tetradecyltrimethylammonium → HCID 20230216, 화합물

HRID 2290750

반응식

HRID 2290750 반응식
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]([C:11]1([N:14]2[CH:18]=[N:17][CH:16]=[N:15]2)[CH2:13][CH2:12]1)=[O:10].[I-].[CH3:20]CCCCCCCCCCCCC[N+](C)(C)C.[OH-].[Na+]>ClC(Cl)(Cl)C>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9]1([C:11]2([N:14]3[CH:18]=[N:17][CH:16]=[N:15]3)[CH2:12][CH2:13]2)[CH2:20][O:10]1

참가 물질

6

반응물 4

HCID 14251TetradecyltrimethylammoniumHCID 14798Sodium HydroxideHCID 30165Iodide IonHCID 212946121-(1H-1,2,4-Triazol-1-yl)cyclopropyl 2,4-dichlorophenyl ketone

생성물 1

HCID 20230216HCID 20230216, 화합물

시약·촉매·용매 1

HCID 62781,1,1-Trichloroethane용매

실험 절차

1-(1-H-1,2,4-Triazol-1-yl)cyclopropyl 2,4-dichlorophenyl ketone (0.5 g, 1.8 mMole) was added to trimethylsulfphoxonium iodide (0.57 g, 2.6 mMole), cetrimide (0.02 g), 1,1,1-trichloroethane (10 ml) and aqueous sodium hydroxide solution (5 ml of 20%). The mixture was refluxed for twenty hours.

후처리

  1. temperatureThe mixture was refluxed for twenty hours

출처 및 근거

ORD 기록
ord-cf1b6c86002a44608be900afac2649bc
출처 데이터셋
uspto-grants-1986_10
특허 번호
US04618616

연결된 노트

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