Cyclohexanone → Prop-2-enenitrile--ethenylbenzene (1/1)
반응식
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][N:2]=1.C1(=O)CCCCC1>CN1CCCC1=O.[Cu]I>[CH2:9]=[CH:10][C:1]#[N:2].[CH2:3]=[CH:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1참가 물질
5
실험 절차
A solution of 2.0 g. CuI, 1.4 g. isoquinoline (1:1 ratio), 50.0 g. N-methylpyrrolidone solvent, 46.6 g. cyclohexanone and 0.20 g. Lustran SAN 31-1,000 (10% on CuI) was prepared. The resulting coating solution was coated on 7 mil raw PET with number 10 Meyer rod and dried three minutes at 240° F. The coating had very good uniformity and clarity and was gold and blue iridescent and lustrous. The resistivity measured 13-20×107 Ω/sq. The solution after time showed some precipitation, which crystals were redissolved upon reheating.
후처리
- customdried three minutes at 240° F
- customsome precipitation, which crystals
- dissolutionwere redissolved
출처 및 근거
- ORD 기록
- ord-3110b0bfc3814e4280160de68cfb5d7b
- 출처 데이터셋
- uspto-grants-1993_11
- 특허 번호
- US05259992
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