N-(2-Chloroethyl)dibenzylamine → HCID 67332185, 화합물

HRID 410992

반응식

HRID 410992 반응식
[CH2:1]([N:8]([CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH2:9][CH2:10]Cl)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH3:19][N:20]([CH3:24])[CH2:21][CH2:22][OH:23].[OH-].[K+]>[Br-].C([N+](CCCC)(CCCC)CCCC)CCC.O1CCOCC1>[CH2:1]([N:8]([CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH2:9][CH2:10][O:23][CH2:22][CH2:21][N:20]([CH3:24])[CH3:19])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

6

반응물 3

HCID 5820N-(2-Chloroethyl)dibenzylamineHCID 79022-(Dimethylamino)ethanolHCID 14797Potassium Hydroxide

생성물 1

HCID 67332185HCID 67332185, 화합물

시약·촉매·용매 2

HCID 74236Tetrabutylammonium Bromide촉매HCID 312751,4-Dioxane용매

실험 절차

[2-(2-Dibenzylamino-ethoxy)-ethyl]-dimethyl-amine was prepared following General Procedure S starting from dibenzyl-(2-chloro-ethyl)-amine (640 mg), 2-dimethylamino-ethanol (325 mg), 50% (w/w) KOH solution (3 mL) and tetrabutylammonium bromide (95 mg) in dioxane (3 mL).

출처 및 근거

ORD 기록
ord-4ae372d5b90a419eb5e8acf22be3a170
출처 데이터셋
uspto-grants-2014_06
특허 번호
US08759535B2

연결된 노트

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