홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Hydrogen Bromide → Silver bromide

HRID 436387
노트
인쇄 미리보기

반응식

HRID 436387 반응식
[OH:1][C:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:3].[BrH:13].[Ag:14].[N+]([O-])([O-])=O.[Ag+]>C(OCCCC)(=O)C>[O-:3][C:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:1].[Ag+:14].[Ag:14][Br:13]
참가 물질반응 조건실험 절차출처 및 근거반응 노트

참가 물질

7

반응물 4

HCID 260Hydrogen Bromide2회HCID 2969Decanoic Acid2회HCID 23954SilverHCID 24470Silver Nitrate

생성물 2

HCID 66199Silver bromideHCID 21226017Silver(1+) decanoate

시약·촉매·용매 1

HCID 31272
Butyl Acetate
용매

반응 조건

온도
5 °C

실험 절차

Into a solution of 8.6 g of capric acid in 100 ml of butyl acetate was emulsified 20 ml of a 2.5%, by weight, aqueous solution of hydrogen bromide while stirring with a stirrer at 5° C. To this emulsion was added 50 ml of an aqueous silver ammine complex solution containing 8.5 g of silver nitrate (which solution had been previously cooled to 5° C) over a period of 30 seconds to allow the capric acid, the hydrogen bromide and the silver ion to react simultaneously to form silver caprate and silver bromide simultaneously. After being allowed to stand, the mixture separated into a water phase and butyl acetate phase containing silver bromide and silver caprate. The water phase was removed and the butyl acetate phase was dispersed into 120 g of a 15%, by weight, solution of polyvinyl butyral in isopropanol. To the resulting silver salt-polymer dispersion, the following components were added in succession at 40° C at intervals of 5 minutes.

출처 및 근거

ORD 기록
ord-dc9fb8b6aef54ceb8431b22ba0b14c3f
출처 데이터셋
uspto-grants-1977_02
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04009039

반응 노트

불러오는 중…

이 페이지에서참가 물질반응 조건실험 절차출처 및 근거반응 노트