Hydrochloric Acid → HCID 178421680, 화합물

HRID 46798

반응식

HRID 46798 반응식
C(N[C:6](=[O:13])[C:7]([C:9]1([CH3:12])[CH2:11][CH2:10]1)=O)(C)(C)C.[NH2:14][NH:15][C:16]([NH:18][NH2:19])=[S:17].Cl.C(O)C>O>[NH2:14][N:15]1[C:6](=[O:13])[C:7]([C:9]2([CH3:12])[CH2:11][CH2:10]2)=[N:19][N:18]=[C:16]1[SH:17]

참가 물질

6

반응물 4

HCID 313Hydrochloric AcidHCID 702EthanolHCID 2724189ThiocarbohydrazideHCID 20385839(1-Methylcyclopropyl)-glyoxylic acid tert-butylamide

생성물 1

HCID 178421680HCID 178421680, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

183 grams of (1-methyl-cyclopropyl)-glyoxalic acid-tert.-butylamide and 112 grams of thiocarbohydrazide were added to a mixture of 1 liter of 1 normal HCl and 1 liter of ethanol. The mixture was boiled under reflux for 8 hours, cooled, diluted with 2 liters of water and the crystals filtered off with suction. There were obtained white crystals with a yellow luster which were dried.

후처리

  1. temperatureunder reflux for 8 hours
  2. temperaturecooled
  3. filtrationthe crystals filtered off with suction
  4. customThere were obtained white crystals with a yellow luster which
  5. customwere dried

출처 및 근거

ORD 기록
ord-e471648b4ae44be4b25f0eae45b4618f
출처 데이터셋
uspto-grants-1979_11
특허 번호
US04175188

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