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Glycine → HCID 10176752, 화합물

HRID 569935
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HRID 569935 반응식
[NH2:1][CH2:2][C:3]([OH:5])=[O:4].[C:6](Cl)(=[O:15])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14].[OH-].[Na+]>O.CCOCC>[C:6]([NH:1][CH2:2][C:3]([OH:5])=[O:4])(=[O:15])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH3:14]
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참가 물질

6

반응물 3

HCID 750GlycineHCID 14798Sodium HydroxideHCID 69819Nonanoyl chloride

생성물 1

HCID 10176752HCID 10176752, 화합물수율 79.5%

시약·촉매·용매 2

HCID 962Water용매HCID 3283Diethyl Ether용매

실험 절차

Glycine (20 mmol) was reacted with nonanoyl chloride (22 ml) in the presence of NaOH (40 mmol) in a mixture of water and ether as described in Example 1 Part A. The crude crystalline product (4.25 g) was recrystallized from ethyl acetate (40-50 ml) to give the title compound (3.42 g, 79.5%), m.p. 106°-109° C.

후처리

  1. customThe crude crystalline product (4.25 g) was recrystallized from ethyl acetate (40-50 ml)

출처 및 근거

ORD 기록
ord-53df7cdd58d64abcbaffbf5a5604cb7b
출처 데이터셋
uspto-grants-1988_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04734424

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