Hydrochloric Acid → HCID 70477797, 화합물

HRID 615308

반응식

HRID 615308 반응식
[Cl-].[Al+3].[Cl-].[Cl-].[C:5](Cl)(=[O:7])[CH3:6].C(Cl)(Cl)(Cl)Cl.[Al+3].[Cl-].[Cl-].[Cl-].[C:18]1([CH:24]([CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH3:43])[C:25]([OH:27])=[O:26])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.Cl>C(Cl)(Cl)(Cl)Cl>[C:5]([C:24]([C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1)([CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH3:43])[C:25]([OH:27])=[O:26])(=[O:7])[CH3:6]

참가 물질

7

반응물 5

HCID 313Hydrochloric AcidHCID 6367Acetyl chlorideHCID 6451240Aluminum(III) ChlorideHCID 220152372-Phenyloctadecanoic acidHCID 131714100HCID 131714100, 화합물

생성물 1

HCID 70477797HCID 70477797, 화합물

시약·촉매·용매 1

HCID 5943Carbon Tetrachloride용매3회

실험 절차

A 500 ml reaction vessel was charged with 200 mls freshly distilled carbon tetrachloride and the CCl4 was cooled to 0°-5° C. Aluminum chloride (0.33 moles) was added, via Gooch tubing, to the CCl4 over a period of 20 minutes. Acetyl chloride (0.35 mol) was added to an addition funnel and charged to the CCl4 -AlCl3 mixture. Phenylstearic acid (0.125 moles) was then slowly added to the reaction mixture from an addition funnel while maintaining the temperature of the reaction mixture at 0°-5° C. The temperature was maintained at 0°-5° C. for one hour and at room temperature for an additional two hours. The evolution of HCl was observed.

후처리

  1. customA 500 ml reaction vessel
  2. temperaturewhile maintaining the temperature of the reaction mixture at 0°-5° C

출처 및 근거

ORD 기록
ord-81c1187f66ae4a17949542ab91d3be67
출처 데이터셋
uspto-grants-1985_02
특허 번호
US04499013

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