N-bromobutanimide → 2-(2,2-Dichlorovinyl)-benzyl bromide
반응식
[Cl:1][C:2]([Cl:11])=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[CH3:10].[Br:12]N1C(=O)CCC1=O>ClC(Cl)(Cl)C>[Cl:1][C:2]([Cl:11])=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[CH2:10][Br:12]참가 물질
4
실험 절차
211 g (1.13 moles) of 2-(2,2-dichlorovinyl)-toluene, 251 g (1.41 moles) of N-bromosuccinimide and 2 g of azoisobutyronitrile in 1300 ml of dry 1,1,1-trichloroethane are refluxed, an additional 1 g of azoisobutyronitrile is added to the reaction mixture after one hour, and heating is continued for a further hour.
후처리
- temperatureheating
- waitis continued for a further hour
출처 및 근거
- ORD 기록
- ord-760ebf0ea2264cd3a5e2e56550388425
- 출처 데이터셋
- uspto-grants-1986_09
- 특허 번호
- US04611010
반응 노트
불러오는 중…