Benzoyl chloride → Methyl Benzoate
반응식
C(Cl)(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:10](=O)([O:13][CH3:14])[O:11]C>S1(CCCC1)(=O)=O.[Cl-].[Li+]>[C:10]([O:13][CH3:14])(=[O:11])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1참가 물질
5
반응 조건
- 온도
- 150 °C
실험 절차
The following example illustrates the use of alkali halide catalysts. A mixture of benzoyl chloride (7.03 g, 0.05 mole), dimethyl carbonate (4.5 g, 0.05 mole) and lithium chloride (0.106 g, 0.0025 mole) in 25 ml of sulfolane was heated to 150° C. for 22 hours. Distillation of the reaction mixture gave 4.77 g (70 percent yield) methyl benzoate.
후처리
- distillationDistillation of the reaction mixture
출처 및 근거
- ORD 기록
- ord-ee2e26d06a894ead8746b98001a992e8
- 출처 데이터셋
- uspto-grants-1986_09
- 특허 번호
- US04612386
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