2,3-Dinitrophenol → Sodium dinitrophenolate

HRID 877867

반응식

HRID 877867 반응식
[N+:1]([C:4]1[C:5]([N+:11]([O-:13])=[O:12])=[C:6]([OH:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[H-].[Na+:15]>C1COCC1>[N+:1]([C:4]1[C:5]([N+:11]([O-:13])=[O:12])=[C:6]([O-:10])[CH:7]=[CH:8][CH:9]=1)([O-:3])=[O:2].[Na+:15]

참가 물질

4

반응물 2

HCID 61912,3-DinitrophenolHCID 24758Sodium hydride

생성물 1

HCID 86649331Sodium dinitrophenolate

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

The anhydrous dinitrophenol (10.0 g, 54.3 mmol) was dissolved in anhydrous THF (300 mL) and then NaH (1.30 g, 54.3 mmol) was added slowly. After the solution was stirred for 3 hrs, solvent was removed under the reduced pressure to obtain 100 mol % sodium dinitrophenolate.

후처리

  1. customsolvent was removed under the reduced pressure

출처 및 근거

ORD 기록
ord-bb64b922e5af466a87709b09e9ad12cb
출처 데이터셋
uspto-grants-2015_03
특허 번호
US08987411B2

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