反应详情

Urocanic acid (138 mg, 1 mmol) was dissolved in dist THF, and a condensing agent CDI (200 mg, 1.3 mmol) was added to this solution. The solution was stirred. After two hours, 2Q (278 mg, 1 mmol) dissolved in dist THF was added and continued to be stirred. After reaction overnight, the reaction solution was filtered through a Kiriyama funnel. The filtrate was concentrated under a reduced pressure to give a yellow oil and this oil was purified by HPLC. Yield: 31%.

1. additionwas added
2. stirringto be stirred
3. customAfter reaction overnight
4. filtrationthe reaction solution was filtered through a Kiriyama funnel
5. concentrationThe filtrate was concentrated under a reduced pressure
6. customto give a yellow oil
7. customthis oil was purified by HPLC