HRID1010795

反应详情

EQUATION

反应方程式

HRID 1010795 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The compound (B) (100 mg) was mixed with 2-Bromoethanol (100 mg) and K2CO3 (120 mg) in Acetonitrile. The reaction was refluxed overnight and filtered, the filtrate was evaporated and purified on silica gel column to give the titled product. Mass: (M+1), 200

WORKUP

后处理

  1. temperatureThe reaction was refluxed overnight
  2. filtrationfiltered
  3. customthe filtrate was evaporated
  4. custompurified on silica gel column