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HRID10425

反应详情

EQUATION

反应方程式

HRID 10425 的结构方程式

REACTANTS

反应物

2
结构：Clc1nc(Cl)nc(Cl)n1
HCID7954

2,4,6-Trichloro-s-triazine

C3Cl3N3

结构：CC(C)(C)OC(=O)N[C@@H]1C[C@@H]2CC[C@@H](C(N)=O)N2C1=O
HCID90895673

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N[C@@H]1C[C@@H]2CC[C@@H](C#N)N2C1=O
HCID91321587

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

100 mg of tert-butyl ((2R,5S,7aS)-5-carbamoyl-3-oxohexahydropyrrolizin-2-yl)carbamate were dissolved in 2 ml of dimethylformamide, and 65 mg of cyanuric chloride were added. The mixture was stirred for 3 h, and the dimethylformamide was removed in vacuo. The residue was chromatographed on silica gel.

WORKUP

后处理

  1. customthe dimethylformamide was removed in vacuo
  2. customThe residue was chromatographed on silica gel