HRID1074380

反应详情

EQUATION

反应方程式

HRID 1074380 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

2.25 Parts of methyl dichlorosilane, 4.04 parts of 1-decene and a solution containing about 0.0005 part of chloroplatinic acid catalyst in 0.006 part of 2-propanol were charged to a reaction vessel and heated to about 100°-120° C. for six hours. The product was vacuum distilled in 110°-114° C. at 1-3 Torr. 4.7 Parts (94% yield) of methyl decyl dichlorosilane was obtained.

WORKUP

后处理

  1. additionwere charged to a reaction vessel
  2. temperatureheated to about 100°-120° C. for six hours
  3. distillationdistilled in 110°-114° C. at 1-3 Torr