HRID1085250

反应详情

EQUATION

反应方程式

HRID 1085250 的结构方程式

PROCEDURE

实验过程

To 15 ml of isopropanol were added 3.0 g of the above prepared compound 11, 3.2 g of 1,3-dimethyl-6-(piperazine-1-yl)-2,4(1H,3H)-pyrimidinedione (compound 2) and 4.2 ml of triethylamine, and the resulting mixture was then treated by the same procedure as in Example 2 in order to obtain 2.2 g of 1,3-dimethyl-6-{4-[2-(2-nitrophenyl)ethyl]piperazin-1-yl}-2,4(1H,3H)-pyrimidinedione.

WORKUP

后处理

  1. additionthe resulting mixture was then treated by the same procedure as in Example 2 in order