huagongshe.com
HRID1085259

反应详情

EQUATION

反应方程式

HRID 1085259 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C(NCCBr)c1ccc([N+](=O)[O-])cc1
HCID458985

未命名化合物

结构：Cn1c(N2CCNCC2)cc(=O)n(C)c1=O
HCID12816873

1,3-Dimethyl-6-(piperazin-1-yl)pyrimidine-2,4(1H,3H)-dione

C10H16N4O2

PRODUCTS

生成物

2
结构：Cn1c(N2CCNCC2)cc(=O)n(C)c1=O
HCID12816873

1,3-Dimethyl-6-(piperazin-1-yl)pyrimidine-2,4(1H,3H)-dione

C10H16N4O2

结构：Cn1c(N2CCN(c3ccc([N+](=O)[O-])cc3)CC2)cc(=O)n(C)c1=O
HCID20061078

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

A mixture of 1.3 g of the compound 46 obtained in the paragraph (1), 1.8 g of 1,3-dimethyl-6-(1-piperazinyl)-2,4(1H,3H)pyrimidinedione (compound 37), 1.3 ml of triethylamine and 10 ml of isopropanol was heated under reflux for 3 hours.