HRID1085313

反应详情

EQUATION

反应方程式

HRID 1085313 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

Reaction and after-treatment were carried out in the same manner as in Example 16 except that an equimolar amount of furfural was used in place of 5-methylfurfural, and that cetyltrimethylammonium chloride and tetrahydrofuran were used in place of tetrabutylammonium bromide and toluene, respectively, in the same weights as those of the latter, to obtain 44.0 g of the fraction of 2-(1-hydroxy-3-butynyl)furan (content, 99.4%) (yield, 80.3%).

WORKUP

后处理

  1. customReaction