HRID1085314
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Reaction and after-treatment were carried out in the same manner as in Example 18 except that an equimolar amount of furfural was used in place of 5-methylfurfural, and that cetyltrimethylammonium chloride and tetrahydrofuran were used in place of tetrabutylammonium bromide and toluene, respectively, in the same weights as those of the latter, to obtain 50.1 g of the fraction of 2-(1-hydroxy-3-butynyl)furan (content, 99.4%) (yield, 91.4%).
WORKUP
后处理
- customReaction