HRID1107515

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID313

Hydrochloric Acid

ClH

结构：CCN(CC)CC(c1cccc2c(C)c(C)oc12)N(CC)CC

HCID18787512

未命名化合物

PRODUCTS

生成物

结构：CCN(CC)CC(c1cccc2c(C)c(C)oc12)N(CC)CC.Cl

HCID18787517

未命名化合物

收率 88%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

400 mg of 2,3-dimethyl-7-[1,2-di(diethylamino)ethyl]benzofuran and 10 ml of a solution of hydrochloric acid in isopropanol are placed in a 100 ml round-bottomed flask. The salt is concentrated under vacuum and recrystallized from ethyl acetate. 400 mg (Yield: 88%) of 2,3-dimethyl-7-[1,2-di(diethylamino)ethyl]benzofuran hydrochloride are obtained. M.p.=183° C.

WORKUP

后处理

concentrationThe salt is concentrated under vacuum
customrecrystallized from ethyl acetate