HRID1156089

反应详情

EQUATION

反应方程式

HRID 1156089 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In reaction (1), o-aminobenzhydrazide in 70% yield is prepared by reacting the methyl ester of o-amino benzoic acid (methyl anthranilate) with 64% aqueous hydrazine. Equation (2) illustrates the preparation of 2-hydroxy-1-naphthaladehyde from beta-naphthol, paraformaldehyde, hexamethylene tetramine, acetic acid and hydrochloric acid. o-Aminobenzhydrazide and 2-hydroxy-1-naphthaldehyde are reacted, in Equation (3), to produce the preferred hydrazone, 2-hydroxy-1-naphthaldehyde-o-aminobenzoyl hydrazone in 80-90% yield.

WORKUP

后处理

  1. customis prepared