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HRID1161522

反应详情

EQUATION

反应方程式

HRID 1161522 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：COC(=O)c1sccc1NN
HCID2777595

Methyl 3-Hydrazinothiophene-2-Carboxylate

C6H8N2O2S

结构：COC(=O)N=C(SC)C(=Nc1ccc(C#N)cc1)c1cc(OC)c2c(c1F)OCCO2
HCID72312729

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1sccc1-n1nc(C(Nc2ccc(C#N)cc2)c2cc(OC)c3c(c2F)OCCO3)[nH]c1=O
HCID135982145

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

CONDITIONS

反应条件

温度
85 °C

PROCEDURE

实验过程

To a solution of 2 g of [2-(4-cyanophenylimino)-2-(5-fluoro-8-methoxy-2,3-dihydrobenzo[1,4]dioxin-6-yl)-1-methylsulfanylethylidene]carbamic acid methyl ester in 24 ml of DMF there were added 720 mg of 3-hydrazinothiophene-2-carboxylic acid methyl ester and 1.2 ml of triethylamine, and the mixture was stirred overnight at 85° C. under a nitrogen atmosphere.