Triethylamine → 1,2-Bis(4-(2-propyl)phenyl)acetylene

HRID 117396Notes

Reaction equation

HRID 117396 reaction equation
[CH3:22][CH2:23][N:24]([CH2:25][CH3:26])[CH2:27][CH3:28].[CH:1]([CH3:2])([CH3:3])[c:4]1[cH:5][cH:6][c:7]([C:10]#[CH:11])[cH:8][cH:9]1.[Cu:70][I:71].[I:12][c:13]1[cH:14][cH:15][c:16]([CH:19]([CH3:20])[CH3:21])[cH:17][cH:18]1.[Pd:29]([Cl:30])[Cl:31].[c:32]1([P:33]([c:34]2[cH:35][cH:36][cH:37][cH:38][cH:39]2)[c:40]2[cH:41][cH:42][cH:43][cH:44][cH:45]2)[cH:46][cH:47][cH:48][cH:49][cH:50]1.[c:51]1([P:52]([c:53]2[cH:54][cH:55][cH:56][cH:57][cH:58]2)[c:59]2[cH:60][cH:61][cH:62][cH:63][cH:64]2)[cH:65][cH:66][cH:67][cH:68][cH:69]1>>[CH:1]([CH3:2])([CH3:3])[c:4]1[cH:5][cH:6][c:7]([C:10]#[C:11][c:13]2[cH:14][cH:15][c:16]([CH:19]([CH3:20])[CH3:21])[cH:17][cH:18]2)[cH:8][cH:9]1

Participants

7

Reactant 6

HCID 8471TriethylamineHCID 11776Triphenylphosphine2×HCID 24290Palladium ChlorideHCID 24350Copper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI)HCID 87073p-IodocumeneHCID 6375011-Ethynyl-4-(1-methylethyl)benzene

Product 1

HCID 112540441,2-Bis(4-(2-propyl)phenyl)acetylene

Sources & evidence

ORD record
ord-2dc62bf57d1f402fb588c6675582e89d
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (2/10)

Reaction notes

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