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HRID1182884

反应详情

EQUATION

反应方程式

HRID 1182884 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)OC(=O)N1CC[C@H](ON)C1
HCID59596622

未命名化合物

PRODUCTS

生成物

1
结构：Cl.Cl.NO[C@H]1CCNC1
HCID68728672

未命名化合物

收率 73%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

(S)-1-tert-Butoxycarbonyl-3-pyrrolidinyloxyamine (1.67 g) was dissolved in a 5M HCl solution in EtOAc (20 ml). After 1 h the solvent was removed under reduced pressure to give (S)-3-pyrrolidinyloxyamine dihydrochloride (1.04 g, 73%) as an off-white solid.

WORKUP

后处理

  1. customAfter 1 h the solvent was removed under reduced pressure