反应详情

334 g (1 mol) of 2-(4-hydroxyphenyl)-2-(4-methylphenyl)hexafluoropropane were dissolved in 1.5 dm3 of dimethylformamide, 276 g of potassium carbonate and 170 g (1.01 mol) of m-dinitrobenzene were added, and the mixture was refluxed for 24 hours. The dimethylformamide was subsequently removed by distillation, and the residue was recrystallized from methanol.

1. temperaturethe mixture was refluxed for 24 hours
2. customThe dimethylformamide was subsequently removed by distillation
3. customthe residue was recrystallized from methanol