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HRID1198056

反应详情

EQUATION

反应方程式

HRID 1198056 的结构方程式

REACTANTS

反应物

5
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C(n1ccnc1)n1ccnc1
HCID68263

1,1'-Carbonylbis(1H-imidazole)

C7H6N4O

结构：[Cl-].[Cl-].[Mg+2]
HCID5360315

Magnesium Chloride

Cl2Mg

结构：CCCCCCCCCCCCS(=O)(=O)CCCC(=O)O
HCID11001756

Butanoic acid, 4-(dodecylsulfonyl)-

C16H32O4S

结构：CC[K].O=C(O)CC(=O)O
HCID178461627

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCS(=O)(=O)CCCC(=O)CC(=O)OCC
HCID53911555

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(dodecylsulfonyl)butanoic acid (H. Gilman, et al, J. Am Chem. Soc. 74, 4452 (1952)) (2.50 g, 0.07 mol), 1,1'carbonyldiimidazole (1.50 g, 0.09 mol), magnesium chloride (1.41 g, 0.014 mol), ethyl potassium malonate (2.12 g, 0.012 mol), and triethylamine (1.73 g, 0.017 mol) using the procedure described in Example 3, Step A.